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As chemical data were generated, checks were made to ensure accuracy (certified reference materials) and precision (repeat measurements) were within accepted tolerance limits. We also ensured measured values fit within those of calibration standards and, if necessary, re-analysed samples diluted to fall within the calibration range. For data generated via mass spectrometry, beam areas of all measured mass-to-charge ratios were corrected for drift offline using control standards. All data were checked to ensure reported values were above the detection limit of the method. 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